Determination Of Softening Point

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Written by Help The Engineer Team
Reviewed by Er. Inderjit Sharma (Retd.), Punjab PWD

What is the softening point? Bitumen doesn’t melt at one exact temperature; it slowly becomes softer as it warms. The softening point is the temperature at which a bitumen disc, carrying a small steel ball, sags 25 mm under standard heating.

Higher softening point = bitumen stays firm at higher temperatures, so the road resists softening, rutting and bleeding in summer.

This is the Ring and Ball test, as per IS 1205.

How the Test Works

1. Start (5 °C)bitumen firm, ball on top2. Warmingbitumen sags under the ball3. Softening pointtouches plate 25 mm below25 mm
Fig. 1: As the bath warms, the bitumen softens and the ball pushes it down. The softening point is the temperature when it touches the plate 25 mm below.

The Ring and Ball Apparatus

25 mm Thermometer Stirrer Ball guide Steel ball 9.5 mm, 3.5 g Brass ring + bitumen Bottom plate Water (≤ 80 °C)or glycerine Heat at 5 °C per minute
Fig. 2: Two brass rings filled with bitumen, each with a steel ball, sit in a glass beaker of water. The bottom plate is 25 mm below the rings.

Apparatus Required

Brass rings (2)

Shouldered rings, 6.4 mm deep, about 16–17.5 mm inside.

Steel balls (2)

9.5 mm diameter, 3.5 ± 0.05 g each.

Ball guides & support

Hold the rings; bottom plate exactly 25 mm below.

Glass beaker

Heat-resistant; at least 85 mm wide and 120 mm deep.

Thermometer & stirrer

Read temperature; keep the bath even.

Heater & stopwatch

Control a 5 °C per minute rise; check every minute.

Procedure

Step 1: Prepare the Specimens

  1. Heat the bitumen to 75–100 °C above its expected softening point. Stir until it is fully fluid and free of air bubbles and water (strain through IS sieve 30 if needed).
  2. Warm the two rings and place them on a metal plate coated with a glycerine–dextrin mixture (to stop sticking).
  3. Fill the rings with bitumen so there is a small excess above the top. Let them cool in air for 30 minutes.
  4. Cut off the excess with a warm knife so the bitumen is level with the ring top.

Step 2: Run the Test

  1. Assemble the rings, ball guides and thermometer in the support, with the bottom plate exactly 25 mm below the rings.
  2. Fill the beaker with freshly boiled distilled water (for softening points up to 80 °C) or glycerine (above 80 °C).
  3. Keep the bath at 5 °C for 15 minutes. Place the cooled steel balls (3.5 g each) in the guides on the bitumen.
  4. Heat the bath so the temperature rises at 5 ± 0.5 °C per minute, stirring all the time.
  5. Note the temperature when the bitumen with the ball touches the bottom plate, for each ring.
  6. If the two temperatures differ by more than 1 °C, repeat the test. Otherwise report the mean to the nearest 0.5 °C.
024681012010203040506070balls drop ≈ 52 °C (about 9.5 min)typical range for VG-30Time (minutes)Bath temp (°C)
Fig. 3: Start at 5 °C and heat at 5 °C per minute. For VG-30 bitumen, the balls usually drop at around 47–55 °C.

Try It: Softening Point Calculator

Enter the temperatures at which each ball touched the plate. The values filled in are a worked example.

Check your heating rate

⬇ Download Excel Proforma

Precautions

🔥 Steady 5 °C/min

Check the rise every minute. Heating too fast gives a falsely high softening point. Don’t “average out” a slow start with a fast finish.

🥄 Stir gently

Stir all the time so the temperature is even, but keep the stirrer away from the rings and balls.

📏 Exactly 25 mm

Check the gap between the ring bottoms and the base plate before starting.

💧 Right bath liquid

Use boiled distilled water up to 80 °C (no air bubbles) and glycerine above 80 °C.

Practical Tips for Site Engineers

1. Minimum Softening Point of Paving Bitumen (IS 73)

GradeMin. softening point
VG-1040 °C
VG-2045 °C
VG-3047 °C
VG-4050 °C

Polymer and crumb rubber modified bitumens (IS 15462) have higher requirements. Follow your contract.

2. Good Site Habits

  1. Read it with penetration: low penetration with high softening point = harder bitumen; high penetration with low softening point = softer bitumen. Both should match the grade.
  2. Hot roads need a higher softening point: pavement surfaces in Indian summers can reach 60–70 °C. That’s why harder grades (VG-30/VG-40) or modified binders are used for heavy traffic and hot areas.
  3. Bleeding and rutting in summer? Check the softening point of the binder used, and the bitumen content of the mix.
  4. Test every tanker, along with penetration, and compare with the supplier’s certificate.
  5. Avoid overheating at the plant: it hardens bitumen and changes its properties. Keep storage and mixing temperatures within the specification.

Key Takeaways

  • Softening point = temperature at which a bitumen disc with a 3.5 g ball sags 25 mm (Ring and Ball test).
  • Fill brass rings, cool 30 min, trim; start the bath at 5 °C; heat at 5 ± 0.5 °C per minute.
  • Water up to 80 °C, glycerine above; balls must agree within 1 °C; report the mean to 0.5 °C.
  • Minimum: VG-10 40 °C, VG-20 45 °C, VG-30 47 °C, VG-40 50 °C.
  • On site: read it with penetration; a higher softening point resists summer softening and rutting.

References: IS 1205: Methods for Testing Tar and Bituminous Materials – Determination of Softening Point; IS 73: Paving Bitumen – Specification; IS 15462: Polymer and Rubber Modified Bitumen.

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